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Vanadium Oxymonochloride, VOCl

Vanadium Oxymonochloride, VOCl, can be obtained by heating vanadium trichloride in an atmosphere of carbon dioxide at about 700° C. for several hours:

3VCl3 + 2CO2 = VCl4 + 2VOCl + 2CO.

It can also be prepared by the reduction of vanadium oxytrichloride, VOCl3, in hydrogen at a red heat. It is a flaky, brown, crystalline substance; density at 16° C., 2.824; soluble with difficulty in water but readily soluble in nitric acid.

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