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Ammonium Orthothiovanadate, (NH4)3VS4

Ammonium Orthothiovanadate, (NH4)3VS4, is obtained in rhombic crystals by the action of ammonium hydrosulphide on potassium metavanadate or sodium pyrovanadate solution. It also separates out slowly from an ice-cold saturated solution of ammonium metavanadate in concentrated ammonium hydroxide which has been previously treated with hydrogen sulphide.

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